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Microstructural evolution during hot shear deformation of an extruded fine-grained Mg–Gd–Y–Zr alloy

机译:挤压细晶mg-Gd-Y-Zr合金热剪切变形过程中的组织演变

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摘要

Mg–Gd–Y–Zr alloys are among recently developed Mg alloys having superior mechanical properties at elevated temperatures. Dynamic recrystallization (DRX) and rare earth (RE)-rich particles play important roles in enhancing the high temperature strength of these alloys. Accordingly, the microstructural evolution of a fine grained extruded Mg–5Gd–4Y–0.4Zr alloy was investigated after hot shear deformation in the temperature range of 350–450 °C using the shear punch testing (SPT) method. The results reveal the occurrence of partial dynamic recrystallization at the grain boundaries at 350 °C while the fraction of DRX grains increases with increasing deformation temperature. A fully-recrystallized microstructure was achieved after SPT at 450 °C. The Gd-rich and Y-rich cuboid particles, having typical sizes in the range of ~50 nm to ~3 m, show excellent stability and compatibility after hot shear deformation and these particles enhance the high temperature strength during hot deformation at elevated temperatures. The textural evolution, examined using electron backscattered diffraction (EBSD), revealed a non-fibrous basal DRX texture after SPT which is different from the conventional deformation texture.
机译:Mg-Gd-Y-Zr合金是最近开发的在高温下具有优异机械性能的Mg合金。动态再结晶(DRX)和富含稀土(RE)的颗粒在增强这些合金的高温强度方面起着重要作用。因此,在350-450°C的温度范围内,采用剪切冲头试验(SPT)方法研究了热剪切变形后细晶粒挤压Mg-5Gd-4Y-0.4Zr合金的微观组织演变。结果表明,在350°C时,晶界发生了部分动态再结晶,而DRX晶粒的分数随变形温度的升高而增加。在450°C下进行SPT后,获得了完全重结晶的微观结构。富含Gd和富含Y的长方体颗粒的典型尺寸在〜50 nm至〜3m范围内,在热剪切变形后表现出出色的稳定性和相容性,这些颗粒增强了高温下热变形过程中的高温强度。使用电子背散射衍射(EBSD)检查的组织演变揭示了SPT后的非纤维基底DRX纹理,与传统的变形纹理不同。

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